Two 2,5‐bis(2‐pyridinyl)‐1,3,4‐oxadiazole–metal complexes (M = Cu and Ni)
Identifieur interne : 000B35 ( Main/Exploration ); précédent : 000B34; suivant : 000B36Two 2,5‐bis(2‐pyridinyl)‐1,3,4‐oxadiazole–metal complexes (M = Cu and Ni)
Auteurs : A. Gueddi ; B. Mernari ; M. Giorgi ; M. PierrotSource :
- Acta Crystallographica Section C [ 0108-2701 ] ; 2000-10.
Abstract
The reaction of the diazine ligand 3,5‐bis(2‐pyridinyl)‐1,3,4‐oxadiazole (pod, C12H8N4O), with Cu(CF3SO3)2 or Ni(ClO4)2 afforded the title complexes diaquabis[3,5‐bis(2‐pyridinyl)‐1,3,4‐oxadiazole‐N2,N3]copper(II) bis(trifluoromethanesulfonate), [Cu(pod)2(H2O)2](CF3SO3)2, and diaquabis[3,5‐bis(2‐pyridinyl)‐1,3,4‐oxadiazole‐N2,N3]nickel(II) diperchlorate, [Ni(pod)2(H2O)2](ClO4)2. Both complexes present a crystallographically centrosymmetric mononuclear cation structure which consists of a six‐coordinated CuII or NiII ion with two pod molecules acting as bidentate ligands and two axially coordinated water molecules.
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DOI: 10.1107/S0108270100011707
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